TO catch my Azelf, I just kept on throwing 5 ultra balls, then 5 timer balls, then 5 ultra, then 5 timer etc. etc. (this is what I do with all my legendary Pokemon actually)
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After the events of spear pillar check out all of the lakes and battle uxie and azelf, Mesprit will run away Sargent Pickles response: I caught uxie but defeated azelf by accident and i tried like 20 pokeballs on uxie until i had to use my master ball it just would give in lol but u can catch it :)
Oh Easy! Weak = Pokéball] Weak = Luxary Ball Bit Tougher = Great Ball I used an Ultra Ball Next comes Quick ball Then Heat Ball Nest balls are good Then Net ball Note: ONLY USE 4 AZELF'S OR UXIE'S Master ball Never fails to catch a pokémon! So u need to buy an... ULTRA BALL!
well try to get his health low and use the best balls! like the net ball master ball ultra ball!
I used a Master Ball to catch Palkia, but that was before I knew Uxie, Azelf, and Mesprit were legendary. It all depends on the types of the Pokemon or how long you expect the battle to last. For Water-type or Bug-type legendaries, use Net Balls. For long-lasting battles, use a Timer Ball. For cave or night battles, use a Dusk Ball. (I recommend this for the Generation IV legendary trio, Uxie, Azelf, and Mesprit.) For Water-types, use a Dive Ball. (I'm not sure where you get this.) An overall ball to use would be the Ultra Ball.
After visiting the Spear Pillar, go to Lake Valor and in the cave you should find Azelf. Bring a Pokemon along that has the move Mean Look so the Azelf cannot escape because they will try to teleport away. You probably will have to try multiple times to catch it if you don't have a Master Ball. If you have gone to Lake Valor and failed to catch it...Look on your Poketech and find the app Berry Finder. Then you must chase the Azelf down...it's easier if you just use Mean Look at Lake Valor because it's really hard to find the Azelf after losing it once.