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First, you need to break into Team Galactic's giant warehouse in Veilstone and once you finally make it up to the boss, he'll give you a master ball if you defeat him.

You have to go to the lottery corner. The lady will ask you to draw and if you get the same number as the ticket you will get a master ball. You can do it once a day.

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Q: How do you get master balls in Pokemon Diamond?
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