In the first episode of season 6.
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the second episode.
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season 6 episode 12 i beleive
She returned in a few episode to meet up with Ash Brock May and Max. Season: 7 Episode: 3: The Princess and the Togepi Season: 7 Episode: 4 A Togepi Mirage Season: 7 Episode: 5 Candid Camerupt "If you ever have any questions about Pokemon you just let me know!"
Ash meets May in the episodes that take place in the Sinnoh season during the dubbed season of Pokémon Diamond and Pearl: Battle Dimension. The episode in which Ash and May reunite is the episode that is titled "A Full Course Tag Battle" however she first appears near the end of the episode that is titled "Our Cup Runneth Over." May returns in order to participate in the Wallace Cup which takes place in the episodes that are titled "Staging a Heroes' Welcome" and "Pruning a Passel of Pals."