At the last episode of Diamond and Pearl Ash and his crew stayed at Dawn's house until the afternoon. Dawn was planning to go with Ash but Dawn and Buneary had to go to the Pokemon Fashion thing. This made Priplup mad so it ran away and long story short they found Priplup. At the end Ash and Brock is about to leave Twinleaf and say their goodbyes to Dawn. At the very end Brock and Ash take their own road. Ash go for Pokemon Master and Brock go for Pokemon Doctor.
Im going to miss Pokemon Diamond and Pearl. The new season is Pokemon Black and White this is a link to watch it.
Can't hyperlink so ima put the web address: http://pokemonepisode.org/
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at episode 5 of Pokemon diamond and pearl
The name of the 3rd Episode in Diamond and Pearl was called "When Pokémon Worlds Collide!"
on youtube
If you are talking about the games, Piplup was introduced in Pokemon Diamond and Pearl... Piplup was introduced in the anime Pokemon Diamond and Pearl episode 1, titled "Following a Maiden's Voyage!"
http://www.animecrazy.net/category/more-running-anime/pokemon-diamond-and-pearl/ try this site in a few days