Yes, Enya did sing in Lord of the Rings. She sang "May It Be" for the Fellowship of the Ring.
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The song May It Be, composed by Enya, was released in 2001. It was originally released as part of The Lord of the Rings: The Fellowship of the Ring soundtrack.
If you are asking which women sing the songs played during the credits at the end of the Lord of the Rings movies, there are three different women singing three different songs. The song at the end of The Fellowship of the Ring is "May it Be" performed by Enya. The song at the end of The Two Towers is "Gollum's Song" by Emiliana Torrini. Finally, the Academy Award winning song at the end of The Return of the King is "Into the West" sung by Annie Lennox. See related links for audio/video to each of the songs.
Arwen's song was actually sung by Liv Tyler, the actress that played Arwen in the Lord of the Rings movies.
It is the theme song for two towers.
Only Time by Enya here's the link: http://www.mshepp.com/onlytime.htm