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Actually the type of compound and its molecular structure designates which technique will be more effective.

XRD is used to measure crystalline compounds and provides a quantitative and qualitative analysis of compounds that cannot be measured by other means.XRF is a technique that is used to measure the percentage of metals within inorganic matrices such as cement and metal alloys. XRF is an especially useful research and development tool in construction industries. This technique is extremely useful for determining the make-up of these materials, allowing for higher-quality cements and alloys to be developed.

Disadvantage : XRD has some size limitations. It is much more accurate for measuring large crystalline structures rather than small ones. Small structures that are present only in trace amounts will often go undetected by XRD readings, which can result in skewed results.

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Why use copper in xrd analysis?

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What are the XRD peaks for glass?

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Why sharp peak and diffuse peak are observed in powder XRD?

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What are the applications of cobalt XRD in materials science and how does it contribute to the analysis of crystal structures?

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What is the use of XRD?

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