None episode.
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I think it's episode 132, because it's called "Hitsugaya, Karin, and The Soccer Ball".
Well, It comes back by the next fight which isn't much later, so :( its kinda sad and funny tho that Captain Hitsugaya gets his arm cut off THREE times by episode 300 and it always comes back :P
in episode 161 miroku's past mistake
No. This event has not happened.
Apperently, Hitsugaya did not die. He was only wounded and as you watch and read the series, you see that he is still alive. toushiro hitsugaya, in his human life, died by a plain of ice. he was then reborn in sole socity (hope i spelt that right) and later on, became a shinigami.